European Journal of Mineralogy
European Journal of Mineralogy
European Journal of Mineralogy
Articles | Volume 37, issue 6
Articles | Volume 37, issue 6
https://doi.org/10.5194/ejm-37-877-2025
© Author(s) 2025. This work is distributed under
the Creative Commons Attribution 4.0 License.
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https://doi.org/10.5194/ejm-37-877-2025
© Author(s) 2025. This work is distributed under
the Creative Commons Attribution 4.0 License.
Articles | Volume 37, issue 6
Research article
 | 
25 Nov 2025
Research article |  | 25 Nov 2025

Ordering of tetrahedral and octahedral layers in synthetic lepidolites and Li-muscovites: two-dimensional {1H} → 29Si ∕ 27Al CPMAS HETCOR and {19F} → 29Si ∕ 27Al CPMAS HETCOR spectroscopy

Michael Fechtelkord and Lara Sulcek

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Short summary
Synthetic lepidolites and Li-muscovites have been investigated using two-dimensional cross-polarisation heteronuclear correlation magic-angle-spinning solid-state nuclear magnetic resonance spectroscopic experiments. All results show a related ordering of the tetrahedral and octahedral sheets, with more tetrahedral Al sites close to Al-rich octahedral sites preferably coordinated by OH- anions and Si-rich tetrahedral regions close to Li-rich octahedral sites preferably coordinated by F- anions.
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Experimental mineralogy, petrology, and geochemistry